Rapid
Process Development And Scale-Up Using A Multiple Reactor System.
This article presents case studies that show how computer control
involving parallel synthesis in specially designed reactors,
particularly on
the 25-100 mL scale, can provide significant benefits...
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A
Comparison of Reaction Hazard Screening Techniques.
The requirement for a systematic approach to chemical reaction
screening is described along with a comparision of results from some
commercially available equipment.
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Parallel
Synthesis of High Pressure Reactions
- including catalyst development. The rapid growth in research
activity, especially in the pharmaceutical industry, has led to an
expansion in the range of tools that can be used to quickly identify,
screen, optomise and scale up new processes.
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Monitoring
and Feedback Control of Supersaturation Using ATR-FTIR to Produce an
Active Pharmaceutical Ingredient of a Desired Crystal Size.
Automation, in situ monitoring, and process control tools are
implemented to understand and control the crystallization of an active
pharmaceutical ingredient in development.
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Automated
Measurement of Metastable Zones for Pharmaceutical Compounds.
It is important to know under what conditions crystals will grow but
not nucleate when developing crysallization processes for the
manufacture of pharmaceutical compounds.
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Safe Scaleup of Exothermic Reactions.
Safe scaleup of exothermic chemical reactions poses a challenge that is
often underestimated. Engineers can help themselves meet the challenge
by acquiring a working knowledge of the principles of calorimetry.
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